An inorganic-organic hybrid possessing a two-dimensional Ti-O network and surface ethoxy groups prepared via a reaction of titanium oxychloride with lithium ethoxide

Natsuki Watanabe, Yoshitaka Kamochi, Seiichi Tahara, Nobuhiro Kumada, Yoshiyuki Sugahara

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Abstract

A new layered inorganic-organic hybrid possessing a Ti-O network has been prepared by a reaction between titanium oxychloride (TiOCl) and lithium ethoxide (LiOEt) at 120 °C for 7 days. The XRD analysis indicates that the interlayer distance of TiOCl increases from 0.80 to 1.19nm, and the solid-state 13CNMR spectroscopy and elemental analysis show partial substitution of ethoxy groups for chlorine atoms.

Original languageEnglish
Pages (from-to)244-245
Number of pages2
JournalChemistry Letters
Volume38
Issue number3
DOIs
Publication statusPublished - 2009 Jul 20

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ASJC Scopus subject areas

  • Chemistry(all)

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