Drastic effect of shearing on graphite microtexture: attention and application to Earth science

Yui Kouketsu, Akira Miyake, Yohei Igami, Tomoki Taguchi, Hiroyuki Kagi, Masaki Enami

Research output: Contribution to journalArticlepeer-review

7 Citations (Scopus)

Abstract

The microtexture of graphite exposed on the polished surface was studied using confocal laser scanning microscopy, laser Raman spectroscopy, and focused ion beam–transmission electron microscopy (FIB–TEM) to elucidate the effect on surface condition and crystallinity of graphite by polishing process. The polished surface of the graphite was divided into a flat part with no irregularities and a grooved band with a width of < 1 μm and a depth of < 100 nm. Raman analyses revealed that the original structure of the graphite covered by the host mineral was a well-ordered graphite, whereas the polished graphite at the surface had a reduced crystallinity, particularly in the flat part of the sample. Based on scanning TEM observations of an ultra-thin FIB section, fractures that developed during sample preparation were concentrated in the region extending from the surface to a depth of 1 μm. Furthermore, graphite sheets were peeled away by shearing, with scraped graphite sheets filling in the gap. Our results demonstrate that the original microtexture of graphite was easily deformed by shearing during polishing, and careful attention should be paid to sample preparation. In addition, we also need to pay more attention to the effects of natural shearing such as faulting on the graphite or sheet-like minerals. [Figure not available: see fulltext.].

Original languageEnglish
Article number23
JournalProgress in Earth and Planetary Science
Volume6
Issue number1
DOIs
Publication statusPublished - 2019 Dec 1
Externally publishedYes

Keywords

  • Confocal laser scanning microscope
  • FIB–TEM
  • Fault rock
  • Graphite
  • Microtexture
  • Raman spectroscopy
  • Shearing
  • Sheet-like mineral

ASJC Scopus subject areas

  • Earth and Planetary Sciences(all)

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