Free-standing poly(l-lactic acid) nanofilms loaded with superparamagnetic nanoparticles

Silvia Taccola, Andrea Desii, Virginia Pensabene, Toshinori Fujie, Akihiro Saito, Shinji Takeoka, Paolo Dario, Arianna Menciassi, Virgilio Mattoli

Research output: Contribution to journalArticle

37 Citations (Scopus)

Abstract

Freely suspended nanocomposite thin films based on soft polymers and functional nanostructures have been widely investigated for their potential application as active elements in microdevices. However, most studies are focused on the preparation of nanofilms composed of polyelectrolytes and charged colloidal particles. Here, a new technique for the preparation of poly(l-lactic acid) free-standing nanofilms embeddidng superparamagnetic iron oxide nanoparticles is presented. The fabrication process, based on a spin-coating deposition approach, is described, and the influence of each production parameter on the morphology and magnetic properties of the final structure is investigated. Superparamagnetic free-standing nanofilms were obtained, as evidenced by a magnetization hysteresis measurement performed with a superconducting quantum interference device (SQUID). Nanofilm surface morphology and thickness were evaluated by atomic force microscopy (AFM), and the nanoparticle dispersion inside the composites was investigated by transmission electron microscopy (TEM). These nanofilms, composed of a biodegradable polyester and remotely controllable by external magnetic fields, are promising candidates for many potential applications in the biomedical field.

Original languageEnglish
Pages (from-to)5589-5595
Number of pages7
JournalLangmuir
Volume27
Issue number9
DOIs
Publication statusPublished - 2011 May 3

ASJC Scopus subject areas

  • Materials Science(all)
  • Condensed Matter Physics
  • Surfaces and Interfaces
  • Spectroscopy
  • Electrochemistry

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  • Cite this

    Taccola, S., Desii, A., Pensabene, V., Fujie, T., Saito, A., Takeoka, S., Dario, P., Menciassi, A., & Mattoli, V. (2011). Free-standing poly(l-lactic acid) nanofilms loaded with superparamagnetic nanoparticles. Langmuir, 27(9), 5589-5595. https://doi.org/10.1021/la2004134