Nucleation and nanometric inhomogeneity in niobiogermanate glass

In-situ inelastic light scattering and tem studies

Y. Takahashi, M. Osada, H. Masai, R. Ihara, T. Fujiwara

Research output: Chapter in Book/Report/Conference proceedingConference contribution

Abstract

We performed in-situ inelastic light scattering measurement in KNbGeO 5 glass with a high nucleation ability during heating in order to elucidate nanocrystallization dynamics. The results of the in-situ measurement and TEM observation revealed that nanometric heterogeneous region (∼1-2 nm) consisting of the Nb-richer phase develops, i.e., K3Nb 7O19, at the temperature, in which glassy-supercooled- liquid (SCL) phase-transition occurs, i.e., precursive stage of nanocrystallization. This strongly suggests that evolution of the nanometric Nb-richer phase in the SCL phase corresponds to nucleation in the KNbGeO 5 glass.

Original languageEnglish
Title of host publicationIOP Conference Series: Materials Science and Engineering
Volume18
EditionSYMPOSIUM 8
DOIs
Publication statusPublished - 2011
Externally publishedYes
Event3rd International Congress on Ceramics, ICC3 - Osaka, Japan
Duration: 2010 Nov 142010 Nov 18

Other

Other3rd International Congress on Ceramics, ICC3
CountryJapan
CityOsaka
Period10/11/1410/11/18

Fingerprint

Nanocrystallization
Inelastic scattering
Light scattering
Nucleation
Glass
Liquids
Phase transitions
Transmission electron microscopy
Heating
Temperature

ASJC Scopus subject areas

  • Materials Science(all)
  • Engineering(all)

Cite this

Takahashi, Y., Osada, M., Masai, H., Ihara, R., & Fujiwara, T. (2011). Nucleation and nanometric inhomogeneity in niobiogermanate glass: In-situ inelastic light scattering and tem studies. In IOP Conference Series: Materials Science and Engineering (SYMPOSIUM 8 ed., Vol. 18). [112009] https://doi.org/10.1088/1757-899X/18/11/112009

Nucleation and nanometric inhomogeneity in niobiogermanate glass : In-situ inelastic light scattering and tem studies. / Takahashi, Y.; Osada, M.; Masai, H.; Ihara, R.; Fujiwara, T.

IOP Conference Series: Materials Science and Engineering. Vol. 18 SYMPOSIUM 8. ed. 2011. 112009.

Research output: Chapter in Book/Report/Conference proceedingConference contribution

Takahashi, Y, Osada, M, Masai, H, Ihara, R & Fujiwara, T 2011, Nucleation and nanometric inhomogeneity in niobiogermanate glass: In-situ inelastic light scattering and tem studies. in IOP Conference Series: Materials Science and Engineering. SYMPOSIUM 8 edn, vol. 18, 112009, 3rd International Congress on Ceramics, ICC3, Osaka, Japan, 10/11/14. https://doi.org/10.1088/1757-899X/18/11/112009
Takahashi Y, Osada M, Masai H, Ihara R, Fujiwara T. Nucleation and nanometric inhomogeneity in niobiogermanate glass: In-situ inelastic light scattering and tem studies. In IOP Conference Series: Materials Science and Engineering. SYMPOSIUM 8 ed. Vol. 18. 2011. 112009 https://doi.org/10.1088/1757-899X/18/11/112009
Takahashi, Y. ; Osada, M. ; Masai, H. ; Ihara, R. ; Fujiwara, T. / Nucleation and nanometric inhomogeneity in niobiogermanate glass : In-situ inelastic light scattering and tem studies. IOP Conference Series: Materials Science and Engineering. Vol. 18 SYMPOSIUM 8. ed. 2011.
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