Preparation of α-zirconium phosphate from fluorozirconate and phosphoric acid by liquid-phase deposition

Seiichi Tahara, Yoshie Takakura, Yoshiyuki Sugahara

Research output: Contribution to journalArticle

9 Citations (Scopus)

Abstract

α-Zirconium phosphate (α-ZrP) was prepared by liquid-phase deposition. Boric acid was added to a solution containing [ZrF 6] 2- anions, and phosphoric acid dropwise to cause slow decomposition of [ZrF 6] 2- and the subsequent reaction with H 3PO 4 to form α-ZrP. X-ray diffraction, scanning electron microscopy, solid-state 31P nuclear magnetic resonance spectroscopy, infrared spectroscopy, thermogravimetry, and elemental analyses indicate the formation of single-phase α-ZrP.

Original languageEnglish
Pages (from-to)555-557
Number of pages3
JournalChemistry Letters
Volume41
Issue number5
DOIs
Publication statusPublished - 2012 May 3

ASJC Scopus subject areas

  • Chemistry(all)

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