Aluminum nitride(AIN) was formed by two-step pyrolysis of poly (isopropyliminoalane) in Ar. The product pyrolyzed at 1000°C was an amorphous material. Solid-state 27Al-nuclear magnetic resonance spectroscopy (NMR) showed that an AIN-like structure was present in the product. Heat treatment of the pyrolyzed product at 1600°C yielded crystalline AIN from the amorphous material.
|Number of pages||3|
|Journal||Nippon Seramikkusu Kyokai Gakujutsu Ronbunshi/Journal of the Ceramic Society of Japan|
|Publication status||Published - 1992|
ASJC Scopus subject areas
- Ceramics and Composites
- Condensed Matter Physics
- Materials Chemistry