Establishment of labo-in-a-microdroplet for azo compound synthesis

Daiki Tanaka*, Shunsuke Sawai, Takuo Sugaya, Yoshito Nozaki, Dong Hyun Yoon, Taisuke Isano, Hitoshi Yamagata, Hiroyuki Fujita, Tetsushi Sekiguchi, Takashiro Akitsu, Shuichi Shoji

*この研究の対応する著者

研究成果: Conference contribution

抄録

In this study, microdroplets are regarded as a “small laboratory”, and complex chemical azo compound was firstly synthesis. The synthesis of azo compounds requires accurate pH control. Furthermore, the reaction is accompanied by heat generation. Synthesis applying microdroplets has advantages over temperature control (ice cold→room temperature (23℃)), pH reagent concentration (5.62 molL-1→0.50 molL-1), synthesis time (3,600 sec→4 sec), and recrystallization work was not necessary. The microdroplet rapidly released heat and no side reaction due to heat occurred. The microdroplet method enables accurate pH control and enables highly pure synthesis.

本文言語English
ホスト出版物のタイトル23rd International Conference on Miniaturized Systems for Chemistry and Life Sciences, MicroTAS 2019
出版社Chemical and Biological Microsystems Society
ページ538-539
ページ数2
ISBN(電子版)9781733419000
出版ステータスPublished - 2019
イベント23rd International Conference on Miniaturized Systems for Chemistry and Life Sciences, MicroTAS 2019 - Basel, Switzerland
継続期間: 2019 10 272019 10 31

出版物シリーズ

名前23rd International Conference on Miniaturized Systems for Chemistry and Life Sciences, MicroTAS 2019

Conference

Conference23rd International Conference on Miniaturized Systems for Chemistry and Life Sciences, MicroTAS 2019
国/地域Switzerland
CityBasel
Period19/10/2719/10/31

ASJC Scopus subject areas

  • バイオエンジニアリング
  • 化学工学(その他)

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