Novel organic-inorganic hybrid and organic-free mesoporous niobium oxophosphate synthesized in the presence of an anionic surfactant

Nawal Kishor Mal, Asim Bhaumik, Masahiro Fujiwara, Masahiko Matsukata

研究成果: Article査読

22 被引用数 (Scopus)

抄録

A novel organic-inorganic hybrid mesoporous niobium oxophenylphosphate was synthesized by using supramolecular assembly of sodium dodecylsulfate molecules. X-ray diffraction, transmission electron microscopic image and N2 adsorption data indicated the formation of a wormhole-like disordered mesostructure in the sample. The 13C and 31P MAS NMR, FTIR, UV-visible spectroscopic data and chemical analysis results indicated that all P atoms are attached to phenyl groups directly and these are combined with Nb atoms through O atoms. Calcination of this hybrid material yielded an organic-free mesoporous niobium oxophosphate material.

本文言語English
ページ(範囲)40-45
ページ数6
ジャーナルMicroporous and Mesoporous Materials
93
1-3
DOI
出版ステータスPublished - 2006 7 28

ASJC Scopus subject areas

  • Chemistry(all)
  • Materials Science(all)
  • Condensed Matter Physics
  • Mechanics of Materials

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